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In most installations, process analyzers are dedicated to one process stream, and if the signal is used for closed-loop control, especially if a chromatograph or analyzer with a longer analysis time is used, this is certainly true. With the increasing use of spectroscopic analysis, there's a tendency to having multiple streams connected to one analyzer, though the price is added complexity with the sample system.
When designing an analyzer system, the following points are important considerations:
Note that in this list only the first two bullets relate to the measurement itself. The balance of the list addresses what I refer to as "ancillary systems," since they're not directly in contact with the process. In general, these items are also normally associated with the analyzer housing.
Because on-line analyzers tend to be more complex and large, they usually require environmental protection in housings to ensure reliable operation. Once it's determined that some added environmental protection is required for the analyzer, the first decision that needs to be made is the form of that housing. The IEC 61831 standard defines the following four types of housings:
Air should enter and leave the house by entry and exit ports from outside the classified area. The air intake should be through a stack provided with a weather protection cowl (rain hood), and sourced from a non-hazardous area where corrosive or toxic gases don't occur. The house should be ventilated with air to keep flammable or toxic gases, which are either lighter or heavier than air, out of the house and to dissipate any leakage inside the house. This not only provides sufficient building ventilation, but it also dissipates any gases that may enter the shelter due to leaks from equipment inside the shelter. To insure that hazardous gases don't enter the shelter, the minimum differential pressure under operating conditions should be 25 pascals (0.25 mbar), effectively creating a purged enclosure. It is normal practice to operate at an overpressure of 2 mbar to 5 mbar with a typical air flow of 10 changes/hour.
The air exchange system, which is normally part of the shelter HVAC, will have to be able to:
It should be noted that many substances will reach the short-term exposure limit or asphyxiant levels long before the lower flammable limit value. As a general rule, the overall system design should eliminate or minimize the emission of hazardous or noxious gases and vapors and the possibility of liquid spillage inside the housing.
Despite the 10 air changes/hour requirement and the need to adequately purge any accidental releases, the design of the intake duct and the diameter of the stack should be sized to limit air velocity to a maximum of 15 m/s since higher velocities not only create a feeling of being in a wind inside the shelter, but also can cause quite a bit of noise. Any ducting to the analyzer house which passes through hazardous areas should be leak-tight. Ducting through Zone 1 hazardous areas should be avoided where possible.
All the above needs to occur while the HVAC unit maintains the temperature inside the house within limits specified by the user and required by the analyzer itself. Rate of change of temperature in the building is also a consideration, since some analyzers are affected by and unable to compensate for changes in ambient temperature.The housing needs to be designed to permit maintenance, adjustments and repairs to be carried out quickly and preferably without affecting analyzer operations. All components likely to require attention should be accessible without the aid of portable ladders or other temporary means, and shall have mountings and fittings located so that they are front-accessible. In the case of cabinet-mounted systems, this includes sufficient room within the cabinet for the technicians' hands, tools and light to see what they are doing or working on. All shelters and houses should have unobstructed internal headroom of at least 2 m, as well as a workspace (bench as a minimum) for support staff to perform maintenance tasks.
Dead zones such as corners and trenches that may collect gas should be avoided. One way this is accomplished is to mount the majority of the sample system "outside" the shelter containing the analyzer(s) proper and then putting in restriction orifices to limit the maximum flow rate through the bulkhead in the event of a catastrophic failure. For this reason equipment such as sample conditioning units, gas cylinders, calibration sample containers and laboratory sampling points are normally located outside the housing with appropriate weather protection.
Besides being protected from exposure to gases that may be in the shelter, personnel working with analyzer systems must be protected from injury from other hazards, such as burns (sample or process lines greater than 40 ºC should be insulated), electric shock (proper grounding of all circuits and the building itself) and cuts from exposed sharp edges.
Manual shutdown devices for the incoming power, sample, carrier gas and other potentially hazardous utilities should be clearly identified outside the housing. These isolation devices should be fitted close to the analyzers. Also, a separate shutdown device should be fitted for any associated house ventilation fans.
Fire detection may be provided in the form of smoke or heat detectors and should be included for all liquid service analyzers. Because not all fires burn the same, be sure to select the right type of fire detector, as you may need to use UV and IR detectors, depending on the fluid. Smoke detectors often help detect fires early in the fire cycle, especially for non-fluid materials.
Of course, if something happens while someone is in the shelter, they'll need a safe exit. Outward-opening doors should be provided at both ends of the housing to permit easy escape in an emergency and include safe egress to the unit's muster point. The position, size of doors and access to them should permit removal of equipment housed. Lockable doors should be avoided, or if they are used, the doors must be capable of being opened from the inside in the locked condition, and they should have crash bars. Manual call points should be provided on the outside of the house next to the doors, so operators can initiate an alarm should the automated systems fail.
Protecting your analyzer investment involves more than "just putting the equipment in a box," regardless of the size and type of box. It also includes providing a safe work environment for the people required to keep that equipment in good working order so that you continue to get highly reliable process analyzer systems as well.