Q: I want to specify an instrument for continuous level measurement in a small cylindrical process vessel with an internal agitator. The internal diameter of the vessel is 632 mm, height is 800 mm, and the measured range is 700mm. There’s a 25-mm nozzle available on top of the reactor for the level transmitter. The process medium is liquid dimethyl sulfoxide (DMSO), having a dielectric constant of 46.4. The conductivity is 3.10 x 10-6 ohm-1 m -1 at 25°. I initially thought about a radar level transmitter, however the dead band on a typical radar transmitter is about 200 mm to 250 mm, and the transmitter would be in close proximity to the vessel wall (multiple echoes). Would an insulated capacitance probe be an option? The agitator is mounted centrally in the vessel and would not come into contact with a probe.
Christopher Beader
CEL International Ltd, Coventry, U.K.
A: You have at least four options: nuclear, load cell, radar and capacitance, each with its own issues.
Nuclear and load cell are both expensive. Also, nuclear requires a NRC license, and weighing requires flexible joints in the connecting piping.
Capacitance measurement has no dead band, but needs to be calibrated for the fluid in the tank. You also have to check if side-loading forces are high enough to bend or damage the probe. Therefore, anchoring the probe is desirable with both types of probes (capacitance or radar).
You should check if the process fluid includes other liquids with different dielectric constants or with different conductivitivities. Otherwise, the capacitance/RF admittance probes have similar limitations as guided wave radar (GWR) probes when it comes to conductive coating.
Radar is probably the best possibility, but because of the small connection size, you cannot use the non-contact type, because it requires a minimum nozzle size of 1.5 in.
The GWR using a time-domain reflectometry (TDR) design would also be my choice. If the nozzle height is more than 50 mm, the dead band should be no problem, because for near-range measurements, the dead band can be as low as 50 mm, particularly if the liquid is reflective. The dead band requirement is slightly more for a single-rod TDR than for the coaxial, but if you include the false signal suppression function, it should enable closer measurement. Your dielectric constant is high enough for GDR measurement if no coating will occur. Proximity to the wall is no problem with the coaxial version because the signal is contained within the tube.
Agitation and the turbulence it causes can cause vibration and mechanical failure, so the probe should probably be secured to the side or bottom of the tank. Check the side loading on the probe tube and make sure the process fluid is clean and free-flowing. The viscosity of 2.14 cP at 20 ˚C should not be a problem. You should also check if the viscosity is constant, or if it changes during the process cycle. As to the type of probe (see Figure 1), I would use the coaxial, because it is the most efficient. It’s efficiency is similar to that of a 75-ohm coaxial cable. If you expect coating, the single-element probe design is the most forgiving.